Hiden Analytical introduce CATLAB, a new integrated
microreactor and mass spectrometer gas analyser for the characterisation
and evaluation of catalysts and for diverse thermal sorption and
reaction studies. The compact, modular system is bench-top mounted
with fully pre-programmable PC control of temperature ramp rate
and setpoint, and of flow rates of up to 8 gas streams.
The microreactor module incorporates an air-cooled fast response
low thermal mass furnace with novel cartridge loading system for
simple reproducible sample placement, the in-bed thermocouple directly
measuring catalyst temperature and reaction exotherms. Close-coupled
sampling direct from the specimen environment minimises dead volume
and memory effects for fast real-time analysis of reaction products
with optimum species resolution.
CATLAB addresses all the needs of the catalyst investigator enabling
characterisation with dynamic TPR/TPO/TPD programs, metal surface
area measurement by N2O decomposition, acidic/basic site quantification
and evaluation, and rapid reproducible screening of catalyst activity
– under identical conditions without sample transfer. |